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The identity of the urinary metabolites of nalfurafine, which is a novel, non-peptide dopamine D2 receptor agonist with both α2- and D1-antagonistic activity, was investigated using high-performance liquid chromatography with ultraviolet detection (HPLC-UV). The separation of the metabolites was performed by a reversed-phase HPLC equipped with a C18 column and a gradient solvent system containing acetonitrile, 0.1% trifluoroacetic acid (TFA) (vol/vol) and 0.1% TFA solution of water for the first 10 min and acetonitrile for the remaining time. Fractions were collected at a rate of 4-5 min/fraction, and were evaluated by thin layer chromatography. Fractions were collected from the gradient solvent system at a rate of 4-5 min/fraction. The structures of the metabolites were determined by comparing their retention times and absorption spectra with those of the synthetic standards and by mass spectrometry (MS). The structures of the metabolites were hydroxylated metabolites, ketone derivatives and sulfate conjugates. Two of the metabolites were found to be more abundant than nalfurafine (5 mg) after administration of a single oral dose of nalfurafine to rats at 20 mg/kg.1. Field of the Invention
The present invention relates to an automatic voltage-adjusting apparatus which automatically adjusts an output voltage in order to compensate for variations in the output voltage of a power supply used for driving integrated circuits, such as liquid crystal display (LCD) panels and plasma display panels (PDP).
2. Description of the Prior Art
Generally, an automatic voltage-adjusting apparatus is included in an integrated circuit device or a semiconductor device, such
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