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with the advent of electron microscopy, nanoparticles can now be measured in the presence of their crystallographic lattice. in this work, convergent-beam electron diffraction (cbed) is successfully applied to measure grains with dimensions in the range of several tens of nanometers. this technique is shown to be capable of determining the grain structure of highly polycrystalline materials, such as aist films prepared by magnetron sputter deposition. cbed reveals the existence of twinning domains, which, as a result, can be used to determine the grain structure of a polycrystalline material. the investigation of the morphology of pedot:pss, poly(3,4-ethylenedioxythiophene) doped with polystyrene sulfonate (pedot:pss), reveals the existence of two domains, where one domain is biaxially oriented and the other is uniaxially aligned to the substrate. the study of the deformation of the electrode surface of a polymer electrolyte membrane, pem, using cbed shows no changes of the lattice symmetry of the membrane when pressurized. this study also supports the findings from other types of measurements, such as fourier transform infrared spectroscopy, which revealed that the crystallinity of the active layer was not influenced by the applied pressure.
we investigate a density functional theory (dft) based methodology for determining the material densities of multicomponent polymeric nanostructures by different elemental compositions. the vaues derived from this approach are compared to the known densities of the same polymers, and it is shown that there is a close relation between the model structure and the atomic compositions of the polymer.
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